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—— Tomo Visava
—— Syed Avais Ali
—— Torikul Zaman
—— Bill
1. Production principle
It can be prepared by the reaction of limestone and hydrochloric acid. The main chemical reactions are as follows:
CaCO3+2HCl→CaCl2+H2O+CO2↑
2. Operation process
1) Calcium chloride dihydrate (CaCl2· 2H2O): Put hydrochloric acid (31%) and limestone powder into the reaction tank at a ratio of 2.2:1, and react under stirring to produce an acidic calcium chloride solution. In the clarification tank. Add lime milk to adjust the pH of the solution to 8.9-9, at this time iron hydroxide and magnesium hydroxide precipitate out. After clarification and filtration, the filtrate is transferred in an evaporating dish and heated to 172~174℃ to evaporate. After crystallization and separation, it is dried and dehydrated at 200~240℃ to obtain calcium chloride dihydrate.
2) Preparation of anhydrous calcium chloride: reheat the dihydrate calcium chloride to 260~300℃, dry and dehydrate, and it will become white anhydrous calcium chloride.
The process of fluidized production of granular calcium chloride is characterized in that liquid calcium chloride is used as a raw material, and the atomized liquid calcium chloride forms a mixed fluidized state with high-temperature hot gas at a temperature of 380-420℃. Under the action of calcium seed crystals, granular anhydrous calcium chloride is obtained.